PREPARATION AND APPLICATION OF MOLECULARLY IMPRINTED FIBER-FILLED NEEDLE TRAP EXTRACTION DEVICE IN REAL SAMPLES
In this study,a needle trap extraction device with a molecularly imprinted polymer coated on Dupont fibers was developed for extraction.A number of heat-resistant Dupont fibers were longitudinally filled into a glass capillary,followed by coating with a molecularly imprinted polymer as an extraction medium and were used to extract volatile organic compounds from environment.Subsequently,the extracted analytes were analyzed by gas chromatography.The linear detection range,recovery,limit of detection(LOD),limit of quantification(LOQ)was studied to evaluate the method.Calibration curves for benzene,toluene,ethylbenzene,and o-xylene were linear in the concentration range of 1–250 μg/L,and the corresponding correlation coefficients exceeded 9897.The LODs and LOQs of the analytes were in the ranges of 15–25 ng/L and 35–65 ng/L,respectively.
Benzene series Needle trap extraction Molecularly imprinted polymer
Xiaoyang Guo Xiyue Wang Bo zhu Lili Lian Hao Zhang Wenxiu Gao Yuanyuan Tian Dawei Lou
Department of Analytical Chemistry,Jilin Institute of chemical Technology,45 Chengde Street,Jilin 132022,PR China
国际会议
吉林
英文
303-305
2018-06-23(万方平台首次上网日期,不代表论文的发表时间)