The Influences of Frequency on the Fabrication and Structural Studies of Micro-Arc Oxidization Ceramic Films Formed on Pure Titanium
The porous oxide TiO2 ceramic film containing Ca and P is fabricated on the surface of pure titanium in the electrolyte of C4H6CaO4-NaH2PO4 by micro-arc oxidation (MAO) method.The microscopic structure, elemental composition and phase components of Ceramic Film are studied with scanning electron microscopy(SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), 3D profilometer and etc.Results indicate that the ceramic film on pure titanium by micro-arc oxidation is a porous mixed crystal structure which contains anatase TiO2 and futile TiO2, and that the film is mainly composed of such elements as Ti, O, Ca and P.With frequency increasing, the number of micropores increases, the hole is decreased in diameter, porosity and roughness, and the surface is more smooth.The increase of frequencies makes the ratio of Ca/P decrease, the relative content of anatase TiO2 increase and rutile TiO2 decrease.
Pure titanium Micro-arc oxidization(MAO) Frequency Microscopic structure Phase composition
Lin Xu Cong Wu Xiao-jing Xu Bo-quan Li Xiao-ya Niu Zhen Huang Jian-ning Ding
School of Mechanical Engineering, Jiangsu University, Zhenjiang 212013, China Changshu Electronic Instrument Factory, Changzhou 215500, China Center of Micro/Nano Science and Technology, Jiangsu University, Zhenjiang 212013, China
国际会议
The 2016 China Functional Materials Technology and Industry Forum (2016中国国际功能材料大会暨第九届中国功能材料及其应用学术会议)
重庆
英文
977-984
2016-07-25(万方平台首次上网日期,不代表论文的发表时间)