Characterization of hydrazinium 3,5-dinitroamine-1,2,4-triazole

摘要：

　　The structure of hydrazinium 3,5-dinitroamine-l,2,4-triazole (HDNAT) was investigated with IR, MS, 13C NMR, SEM and X-ray crystallography.The crystal density of HDNAT was determined as 1.91g/cm3 by using X-ray diffraction.The crystal belongs to monoclinic system with space group P2(1).The thermal decomposition process of HDNAT was investigated via TG-DTA at a heating rate of 10 K/min and DSC under a non-isothermal condition.The decomposition kinetic and thermodynamic parameters were obtained by Kissinger and Ozawa method.HDNAT can be analyzed by using a C18 HPLC column with water/acetonitrile/TFA (97/3/0.1, v/v/v) as mobile phase and a capacity factor of 1.33.

关键词： triazole energetic material hydrazinium 3,5-dinitroamine-1,2,4-triazole characterization

作者: CUI Kejian MENG Zihui XU Zhibin XUE Min LIN Zhihui WANG Bozhou GE Zhongxue QIN Guangmin

作者单位: School of Chemical Engineering and Environment,Beijing Institute of Technology,Beijing 100081,China Xian Modern Chemistry Research Institute,Xian 710065,China

会议类型: 国际会议

会议名称: 2013 International Autumn Seminar on Propellants, Explosives and Pyrotechnics(2013国际推进剂、炸药、烟火技术秋季研讨会)

会议地点: 成都

会议语种:英文

页码: 266-272

在线出版日期: 2013-09-24（万方平台首次上网日期，不代表论文的发表时间）