Characterization of Au Ring Microelectrode with Cyclic Voltammetry and AC Impedance Spectroscopy
In this paper Au ring microelectrodes are fabricated and characterized.With an optical fibre core as a substrate Au film with thickness 300nm was coated by an electron beam evaporation system,then on this Au coated substrate a parylene passivation layer was deposited,forming the desired Au ring microelectrode.Scanning electron microscopy (SEM) was used to characterize the quality of the deposited films and the adhesion at the interfaces.With a CHI660D electrochemical workstation the electrochemical characterizations were performed at room temperature in a conventional three-electrode system.Cyclic voltammograms as a function of scan rate were sigmoidal form,a typical electrochemical response of microelectrodes.AC impedance frequency spectrum of the fabricated Au ring microelectrode was also obtained in a reversible system,and good agreement was found with the Randels-type equivalent circuit.
Electron beam evaporation system Vacuum deposition system Scanning electron microscopy Cyclic voltammetry AC impedance frequency spectrum
Weixuan Jing Fan Zhou Lujia Chen Zhuangde Jiang Lingling Niu Bing Wang Han Qi
State Key Laboratory for Manufacturing Systems Engineering Xian Jiaotong University 710049, Xian, China
国际会议
2013 International Symposium on Assembly and Manufacturing(2013装配与制造国际专题会议)
西安
英文
125-127
2013-07-01(万方平台首次上网日期,不代表论文的发表时间)