Optimization of synthesis of 2-ethoxy-4-nitrophenol

摘要：

　　This paper presents the synthesis of 2-ethoxy-4-nitrophenol using three types of nitrification synthesis schemes with 2-ethoxyphenol as main reactant.The comparison of the reaction conditions,reaction time,the quantity of the reaction byproducts,yield and post-treatment of the reaction product among these three synthesis schemes is made.It concludes that Ferric nitrate is the optimal catalyst for nitrification.Finally,melting point test and infrared characterization were conducted for the products.It shows that the product contains 2-ethoxy-4-nitrophenol and the yield is 55.48%.

关键词： 2-ethoxy-4-nitrophenol Decoquinate Ferric nitrate Synthesis

作者: Zhihui Hao Kefeng Xiao Leilei Wang

作者单位: Laboratory of Bio-pharmacy of Agricultural, Institute of Chemistry and Pharmacy, Qingdao Agricultural University, Qingdao, China, 266109

会议类型: 国际会议

会议名称: 2012 The 2nd International Conference on Biotechnology,Chemial and Materials Engineering(第二届生物、化工和材料工程国际会议(CBCME2012))

会议地点: 厦门

会议语种:英文

页码: 65-68

在线出版日期: 2012-12-28（万方平台首次上网日期，不代表论文的发表时间）