Preparation of L-α-glycerophosphocholine from Natural Lecithin Catalyzed by Tert-butylamine

摘要：

　　Tert-butylamine was confirmed as effective catayst for preparing L-α-glycerophosphocholine at mild conditions.The process using this catalyst would be much simpler,since the recovery of the catalyst can be combined with the recovery of methanol by distillation.The conversion of phosphatidylcholine could reach over 98% after 4 h,with a catalyst content of 2.4% under 60 ℃.The mechanism of the methanolysis reaction was proposed and the experimental data fit the equation model well.GC was used to analyze the product,it was indicated that the product had high purity,and the catalyst could get similar effect to the fresh after repeatedly used.

关键词： L-α-glycerophosphocholine transesterification tert-butylamine natural lecithin

作者: Hongya Li Xiaoli Zhang Weili Bai Binxia Zhao

作者单位: School of Chemical Engineering, Northwest University, Xian 710069, China;School of Chemistry and Ch School of Chemical Engineering, Northwest University, Xian 710069, China Shaanxi Applied Physics and Chemistry Research Institute, Xian 710061, China

会议类型: 国际会议

会议名称: 2012 The 2nd International Conference on Biotechnology,Chemial and Materials Engineering(第二届生物、化工和材料工程国际会议(CBCME2012))

会议地点: 厦门

会议语种:英文

页码: 148-151

在线出版日期: 2012-12-28（万方平台首次上网日期，不代表论文的发表时间）