Methyl Trichlorosilane Prepared Methyl Sodium Silicate

摘要：

　　This paper studied how to prepare Methyl Sodium Silicate from Methyl Trichlorosilane.Methyl trichlorosilane hydrolyzed on the interface of cyclohexane and water,then hydrolysate and sodium hydroxide prepared methyl sodium silicate at molten state.Manufactrue was characterised by XRD,IR,and differential thermal analysis.The experimental results indicate that the best hydrolyze condition was the proportion of methyl trichlorosilane and water was 10~12∶100,at 5℃,lasting for 45min; the best condition of prepared methyl sodium silicate was the proportion of sodium hydroxide and hydrolysate was 2.1~2.3∶1,at 300~450℃,lasting for 50min.The manufacture was white powder,water-solubility and well stabilization bellow 450℃.

关键词： methyl trichlorosilane methyl sodium silicate condensation reaction methyl silicane

作者: Guangxia Zhang Qiaoyun Zhang Zemin Chen

作者单位: Chemistry and Material Science Institute of Langfang Teachers College HeBei 065000 China

会议类型: 国际会议

会议名称: the 2012 International Conference on Frontiers of Mechanical Engineering and Materials Engineering (机械工程与材料工程国际会议())

会议地点: 香港

会议语种:英文

页码: 1064-1067

在线出版日期: 2012-07-27（万方平台首次上网日期，不代表论文的发表时间）