Preparation and Characterization of Anodic Alumina Membrane with Nanopore Arrays
Anodic alumina membranes (AAM) with nanopore arrays were prepared by one-step anodization of highly pure aluminum foil.Morphology,structure and composition of AAM were characterized by scanning electron microscopy (SEM),energy dispersion spectroscopy (EDS),X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD).Results showed that AAM owned honeycomb structure which was characterized by close-packed arrays of columnar hexagonal cells,each containing a central pore normal to the substrate.The diameter of pores and the size of cells changed under different anodic conditions,such as temperature,concentration of H2C2O4 solution,voltage and time ofanodization.The walls of AAM were composed of two strains of nanoparticles of alumina.Furthermore,the chemical composition of AAM was found to be amorphous alumina.The prepared AAM with nanopore arrays is a kind of ideal template for preparation of many one-dimensional nanomaterials.
anodic alumina membrane nanopore array one-step anodization characterization
Xiao-hong Tang Wen-bin Yang Ya-fei Cheng Quan-guo Huang
College of Economics and Management, Southwest University of Science and Technology,Sichuan 621010, State Key Laboratory Cultivation Base for Nonmetal Composite and Functional Materials,Southwest Univ School of Materials Science and Engineering, Southwest University of Science and Technology,Sichuan
国际会议
太原
英文
358-361
2012-06-23(万方平台首次上网日期,不代表论文的发表时间)