Analysis of Permethrin in Cole by Dispersive Solid Phase Extraction

摘要：

　　A new dispersive solid phase extraction (DSPE) method coupled with GC detection was established for determination of permethrin residue in cole.The proposed DSPE method was carried out using acetonitrile as the extraction solvent,and neutral alumina oxide as dispersive adsorbent.The factors that affected DSPE efficiency were validated in terms of extraction solvent,extraction time,and dispersive adsorbent kinds and interaction time.The developed method could give satisfactory recovery (91.2-107.4%) with RSD≤4.9%.Good linearity was observed in the range of 0.005-1.19 mg/g with the correlation coefficients (r2) of 0.9992.The detection limits for permethrin was of 0.43 μg/g.The method had been successfully applied to the analysis of permethrin esidues in cole samples.

关键词： Dispersive solid phase extraction Gas chromatography Permethrin Cole

作者: Fengxia Qiao Mengge Wang

作者单位: Department of Biochemistry,Baoding University,Baoding 071000,China

会议类型: 国际会议

会议名称: the 2012 2nd International Conference on Frontiers of Manufacturing Science and Measuring Technology (第二届制造科学与检测技术国际会议(ICFMM 2012))

会议地点: 西安

会议语种:英文

页码: 1186-1189

在线出版日期: 2012-06-12（万方平台首次上网日期，不代表论文的发表时间）