Selective Synthesis of Boron Nitride Nanotubes
Four types of boron nitride (BN) nanotubes are selectively synthesized by annealing porous precursor in flowing NH3 and NH3/H2 atmosphere at temperature ranging from 1000 to 1200 ℃ in a vertical furnace.The as-synthesized BN nanotubes,including cylinder,wave,bamboo and bubble-chain,are characterized by scanning and transmission electron microscopy.Selectivity of BN nanotubes is estimated as approximately 80 to 95%.The porous precursor B31Fe17(MgO)27 prepared by self-propagation high-temperature synthesis (SHS) method plays a key role in controllable synthesis of the as-grown BN nanotubes.The chemical reaction and annealing mechanism are also discussed.
Boron nitride Nanotubes Chemical vapor deposition Synthesis
Laiping Zhang Jilin Wang Guowei Zhao Zhanhui Zhang Fang Zhang Yunle GU Weimin Wang
School of Material Science and Engineering,Wuhan Institute of Technology,Wuhan 430073,China School of Material Science and Engineering,Wuhan Institute of Technology,Wuhan 430073,China;Nano and The State Key Laboratory of Advanced Technology for Materials Synthesis and Processing,Wuhan Univers
国际会议
大理
英文
408-412
2011-08-18(万方平台首次上网日期,不代表论文的发表时间)