Preparation and characterization of spherical mesoporous material SBA-15 in the presence of H3PO4

摘要：

　　The spherical mesoporous material SBA-15 was synthesized by amphiphilic triblock copolymer P 123 as the template in the presence of phosphoric acid.The samples were characterized by polarizing microscope,N2 adsorption-desorption,XRD and SEM.The experimental conditions were studied in detail.We found that the perfect spherical SBA-15 with a good crystallinity and narrow pore size distribution could be obtained at 4 mol/L phosphoric acid,mild stirring rate,and 10 ℃ reacting temperature.

关键词： H3PO4 SBA-15 sphere shape

作者: Wenjiang Li Zhenyun Yu Fei Xie Meizhou Qi

作者单位: College of Science,State Key Laboratory of Heavy Oil Processing,China University of Petroleum,Qingdao,Shandong,266555,China

会议类型: 国际会议

会议名称: the international conference on Frontier of Nanoscience and Technology (2011纳米科学与技术国际会议(ICFNST 2011))

会议地点: 大理

会议语种:英文

页码: 804-808

在线出版日期: 2011-08-18（万方平台首次上网日期，不代表论文的发表时间）