Preparation and Characterization of LaAlO3 via Sol-gel Process
Lanthanum aluminate powders were synthesized by sol-gel process with metal nitrates as raw materials,2-methoxyethanol/water as solvent and citric acid as chelating agent.The influence of this techniques (the amount of citric acid,pH value,calcination temperature and the ratio of 2-methoxyethanol/water) on the lanthanum aluminate powders were studied.The XRD shows pure LaAlO3 powders could be obtained after calcining at 600-900℃.The SEM analysis indicates that the LaAlO3 particles are uniform and nanosized with a range of about 40-70 nm,which is slightly larger than the estimated particle size using Scherrer formula.
Sol-gel process LaAlO3 powder
Xiaoyan Zhang Teng Zhang Xiwei Qi JianQuan Qi Guifang Sun Huanhuan Chen RuiXia Zhong
School of Resources and Materials,Northeastern University at QinHuangDao Branch,QinHuangDao 066004
国际会议
桂林
英文
26-29
2012-07-16(万方平台首次上网日期,不代表论文的发表时间)