Study on a High-temperature Delayed Cross-linked Acid
A retarded zirconium cross-linking agent ECA-1 was developed by using zirconium oxychloride,citric acid,lactic acid and so on,then we got a high-temperature delayed cross-linking acid with cross-linking agent ECA-1 added to EVA-180 thickening acid,cross-linked acid performance and its influencing factors were discussed in details,such as reaction conditions of crosslinker,concentrations of crosslinker and thickener,and so on.The results showed that the obtained cross-linked acid has good temperature-tolerate and shear-tolerate properties when the mass ratio of zirconium oxychloride,lactic acid and xylitol is 1∶1.25∶0.0208,the reaction temperature is 50~55℃,the reaction time is 4 hours,the delayed cross-linking time of acid system can be adjusted by changing the dosage of crosslinker and thickener.
Organic zirconium crosslinker preparation delayed cross-linking temperature-tolerate and shear-tolerate properties
Xiao Zhao Qi Song Hai Lin Yanling Wang Zengbao Wang Jiafeng Jin Chao Xu
SINOPEC Research Institute of Petroleum Engineering Beijing 100101,P.R.China SINOPEC Petroleum Engineering Technology Research Institute of JOECO Yangzhou 225009,P.R.China Qinghai Oilfield Technology Institute of Drilling & Production,PetroChina Dunhuang 736202,P.R.China College of Petroleum Engineering China University of Petroleum Qingdao 266580,P.R.China
国际会议
桂林
英文
252-255
2012-07-16(万方平台首次上网日期,不代表论文的发表时间)