Synthesis and Characterization the Intercalation Compound of SnS2-Ethylenediamine by Hydrothermal Reaction
The intercalation of ethylenediamine (en) into SnS2 was synthesised by hydrothermal reaction at the temperature of 180℃.And then dispersed the intercalation compounds in N,N-dimethylformamide (DMF) by stirring 48h,getting a light yellow sol,with the nature of uniform,transparent and stable.Analysised the structural of the product by means of X-ray powder diffraction (XRD).The morphology of sol was characterized by using of transmission electron microscopy (TEM).The UV-Vis spectrophotometer was utilized for the absorbance of the colloidal.The results show that en has been successfully inserted into the layer of tin disulphide,and the target products is of high purity and good crystal.The sol is of high stability and homogeneity,and have the strongest absorption at the Wavelength of 270nm.
Tin disulfide Ethylenediamine Intercalation Compound Hydrothermal
Qing Lv Caixia Li Danyu Jiang Qiang Li
Department of Chemistry,East China Normal University,Shanghai 200062,China Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai 200050,China
国际会议
The Seventh China International Conference on High-Performance Ceramics (第七届先进陶瓷国际研讨会(CICC-7))
厦门
英文
215-218
2011-11-04（万方平台首次上网日期，不代表论文的发表时间）