Influence of S/La Molar Ratio on the Morphology and Optical Property of La2S3 Microcrystalline Prepared by Microwave Hydrothermal
The La2S3 microcrystalline was prepared by microwave hydrothermal method (M-H).The influences of S/La molar ratio on the phase composition,and morphology of the La2S3 microcrystalline were particularly investigated.The obtained samples were characterized by X-ray diffraction (XRD),scanning electron microscopy (SEM),ultraviolet and visible spectroscopy (UV-vis) and photoluminescence spectroscopy (PL) at room temperature.With the decrease of S/La molar ratio from 6/3 to 6/6,crystallization of the obtained microcrystalline is improved.The morphology of prepared La2S3 transforms from irregular shapes to quasi-sphere structure.The as-prepared microcrystalline shows excellent absorbency of ultraviolet light and are almost transparent to visible light to exhibit stable violet-blue photoluminescence properties under the ultraviolet light excitation at room temperature.
La2S3 microcrystalline Optical property Microwave hydrothermal
Zhang Ye Cao Li-yun Huang Jian-feng Wu Jian-peng
Key Laboratory of Auxiliary Chemistry & Technology for Light Chemical Industry,Ministry of Education,Shaanxi University of Science & Technology,Xian Shaanxi 710021,China
国际会议
The Seventh China International Conference on High-Performance Ceramics (第七届先进陶瓷国际研讨会(CICC-7))
厦门
英文
223-226
2011-11-04(万方平台首次上网日期,不代表论文的发表时间)