Properties of Mechanical Activation Combustion Synthesied High α-Content Silicon Nitride Powders and Sintered Bulk Ceramics after Iteration Reactions
Effect of iteration times on mechanically-activated combustion synthesis of high α-content Si3N4 powders was investigated.Properties of the as-synthesized powders such as α-content (Ca) as well as specific surface area (As) were examined.Results showed that both of Cα and As became higher after iteration reactions.The mechanical properties of the sintered bulk ceramics from as-synthesized powders were also tested to reveal the sinterability of the powders.Results showed that relative density of all the sintered bulk ceramics were higher than 97%.Furthermore,fracture toughness had a trend of becoming higher,which reached a value of 10.2 MPam 0.5.Correspondingly,bending strenth became a bit lower.
Silicon nitride Mechanically-activated combustion synthesis Mechanical properties
Ren Kegang Chen Kexin Zhou Heping Jin Haibo Zhong Jidong Ning Xiaoshan
Department of Materials Science & Engineering,The State Key Lab.of New Ceramics & Fine Processing,Ts School of Materials Science & Engineering,Beijing Institute of Technology,Beijing 100081,China
国际会议
The Fifth China International Conference on High-Performance Ceramics (第五届先进陶瓷国际研讨会(CICC-5))
长沙
英文
862-864
2007-05-10(万方平台首次上网日期,不代表论文的发表时间)