Research on Preparation and Structure of Ca3Co4O9

Ca3Co4O9 particles were synthesized using cobalt nitrate,calcium nitrate,and citric acid as the starting precursors by sol-gel method.The absolute ethyl alcohol was selected as the solvent.LFA447 was applied to measure the thermal conductivity from room temperature to 300℃ as the reference to decide the optimal parameters.And the optimal parameters obtained are as follows: ethyl alcohol 100ml,ethylene glycol 5ml,citric acid 12.11g (the mole ratio of citric acid to metal ions is 1.1∶1),and pH=3 to prepare samples with total weight of 5 g.
Ca3Co4O9 powder Sol-gel method Orthogonal experiment
Weirong Zhang Zhanyong Wang Wenqing Liu
lnstitute of Materials Science, Shanghai University, 149 yanchang Road, Shanghai 200072, China Department of Materials Science and Engineering, Shanghai Institute of Technology, 100 haiquan Road,
国际会议
the Chinese Materials Congress 2012(2012年中国材料大会(CMC2012))
太原
英文
111-115
2012-07-13(万方平台首次上网日期,不代表论文的发表时间)