Hydrothermal Synthesis and Photoluminescence of Pre-Perovskite Lead Titanate Nanofibers
Pre-perovskite PbTiO3 nanofibres were synthesized by hydrothermal method with four butyl titanate ((C4H9O)4Ti) and lead nitrate (Pb(NO3)) as the main precursors and Tetramethylammonium Hydroxide (TMAH) as mineralizer.X-ray diffraction (XRD),Raman,Scanning Electronic Microscopy (SEM),Transmission electron microscopy (TEM),high-resolution TEM (HRTEM),and the corresponding selected area electron diffraction (SEAD) were used to characterize the crystal structure and morphology of the obtained products.The results showed that the nanofibers are of a few to tens micrometer at length size,and 50~300 nm at diameter size.Based on the experimental results,the effect of Tetramethylammonium Hydroxide (TMAH) was simply discussed.
Hydrothermal Pre-perovskite PbTiO3 Single crystal Nanofiber
Junhao He Gang Xu Xiao Wei Zhaohui Ren Ge Shen Gaorong Han
State Key Laboratory of Silicon Materials, Department of Materials Science and Engineering,Zhejiang University, Hangzhou 310027, China
国际会议
the Chinese Materials Congress 2012(2012年中国材料大会(CMC2012))
太原
英文
382-386
2012-07-13(万方平台首次上网日期,不代表论文的发表时间)