Synthesis of Thiadiazole Zineb

摘要：

In this paper, a series of 2-amino-5-alkyl-l, 3, 4-thiadiazole zineb were prepared by reacting 2-amino-5-alkyl-1, 3, 4-thiadiazole, CS2 and ZnCl2.Its synthesis conditions was discussed.The optimal conditions were obtained as follows: reaction time 120 min, reaction temperature 30°C, molar ratio n (thiadiazole): n (zinc chloride): n (CS2): n (NaOH) = 1:1:1.05:1.05, the products was synthesized in water.All compounds were characterized by elemental analysis, Infrared (IR)analysis to determine their structure.

关键词： 2-amino-5-alkyl-l,3,4-thiadiazole zineb carbon disulfide sodium hydroxide synthetic

作者: Liu Yuting Su baojun Zhou Ying Yin Dawei

作者单位: Key laboratory of Auxiliary Chemistry & Technology for Chemical Industry,Ministry of Education,Shaan Key laboratory of Auxiliary Chemistry & Technology for Chemical Industry,Ministry of Education,Shaan

会议类型: 国际会议

会议名称: International Conference on Advances in Engineering 2011(2011年工程研究进展国际学术会议 ICAE2011)

会议地点: 南京

会议语种:英文

页码: 519-522

在线出版日期: 2011-12-17（万方平台首次上网日期，不代表论文的发表时间）