An investigation on the preparation of active carbon-ceramic sphere
A procedure for the preparation of active carbonceramic sphere was developed.Active carbon-ceramic sphere were prepared by coating a porous ceramic sphere with a phenolic resol resin (carbon precursor).The following procedure was adopted: (a) impregnation of the ceramic substrate with phenolic resol resin; (b) curing; (c) carbonization; (d) activation with KOH etching; (d) washing and drying. Under the optimal impregnation conditions, the material obtained (PRR 70 %) at 30°C, which exhibited a high carbon percentage (~ 5.3 wt.%) with a total pore volume of 0.276 cm3g-l and a specific surface area of 471 m2g-l (carbon in the carbon-ceramic sphere) by N2 adsorption, respectively.By means of chemical activation (KC-120), the total pore volume increased to 0.69 cm3g-l and the specific surface area to 1110 m2g-l (carbon percentage: 4.73 wt.%), respectively.The activated material shows a uniform carbon distribution, good adsorption properties and a high mechanical strength (24MPa).
phenolic resol resin porous ceramics carbon-ceramic sphere active carbon
Liu WeiMin Wang Lei Li Shuzhen Chen Yujing Wu xihui
School of Chemical and Environmental Engineering,Shanghai Institute of Technology ShangHai,200235,P.R.China
国际会议
厦门
英文
98-102
2011-07-08(万方平台首次上网日期,不代表论文的发表时间)