Solvothermal Synthesis and Characterization of Two Iron Complexes

摘要：

Two iron complexes, Fe3(dtdb)2)(HCO2) 2(DMF)2(H2O)2(1)and Fe(bpy)(Hdtdb)(H2O) (2) were solvothermally synthesized and characterized by single crystal X-ray diffraction. Fe3(dtdb)2(HCO2)2(DMF)2(H2O)2(1) shows 2D layer structure crystallized in a triclinic with space group P-1 and cell parameters, a=8.5591(10) nm, b=11.2502(13) nm, c=11.4370(14) nm, a=90.687(2)°,β=110.275(2)° ,γ=90.712(2)°, and Z=1. Fe(bpy)(Hdtdb)(H2O) (2) shows surper-molecular architecture crystallized in a triclinic with space group P-l and cell parameters, a=8.286(12) nm, b=11.5937(16) nm, c=11.8477(17) nm, α=93.932(3)°, β=102.442(3)°,γ=97.117(3)°,and Z=1.

作者: Yawei Hu Yangmin Ma

作者单位: Key Laboratory of Auxiliary Chemistry Technology for Chemical Industry, Ministry of Education, Shaanxi University of Science and Technology, Xian, Shaanxi 710021, P.R.China

会议类型: 国际会议

会议名称: The Second Annual Meeting on Testing and Evaluation of Inorganic Mateirals(第二届全国无机材料测试与评价学术年会 TEIM-2)

会议地点: 长沙

会议语种:英文

页码: 324-327

在线出版日期: 2011-06-30（万方平台首次上网日期，不代表论文的发表时间）