Preparation crystalline mesoporous titania at mild conditions with inorganic titanium precursors

摘要：

In order to avoid the damage on mesostructure by the high temperature treatment,inorganic titanium species were used as the precursors for the preparation of mesoporous TiO2 of crystalline framework at mild conditions.The influences of the precursor,additive,reaction pH and temperature on phase and textural structures of the products were investigated.The samples were characterized by XRD,N2 adsorption/desorption,FT-IR and SEM.The results show that anatase mesoporous TiO2 with large surface area could be obtained without calcination with Ti(SO4)2 as precursor or TiCl4 when SO42- was added.And the template could be completely removed by Soxhlet extraction.

关键词： mesoporous titania crystalline framework anatase low tempreture synthesis

作者: Zuo Jinlong

作者单位: Department of Environmental Engineering,Harbin University of Commerce,Harbin 150076,China

会议类型: 国际会议

会议名称: 2010 International Conference of Environment Materials and Environment Management(2010年环境材料与环境管理国际学术会议 EMEM 2010)

会议地点: 哈尔滨

会议语种:英文

页码: 2053-2056

在线出版日期: 2010-07-24（万方平台首次上网日期，不代表论文的发表时间）