Dtermination of Trace Tetracycline in Waste-water by Phase-separation Floatation with Ultraviolet Detection

摘要：

A new analytical method was demonstrated for the determination of trace tetracycline (TC) in medicine by phase-separation floatation(PSF) coupled with an ultraviolet detector setting at 383 nm. TC can be transformed into binary complex(Mg-TC) in the conditions of magnesium(II) which can be separated by phase-separation floatation easily. The optimum phase-separation floatation was performed on phaseseparation reagent using 3.5 mol·L-1 sodium chloride, O.Olmol·L-1 sodium hydroxide as acidity regulator and n-propyl alcohol as solvent. The linear regression equation is A=1.912×l05C+ 0.011, linear range is from 1.7×l0-7-1.02×l0-mol·L-1, floating rate is 89.0％,enrichment multiple is 26.7. The recoveries of TC in urine were 96.1-98.2％.

关键词： phase-separation floatation(PSF) Ultraviolet detection tetracycline (TC)

作者: Hou Yan-min Cheng Yong-hua Xie Ji-min

作者单位: School of chemistry and chemical engineering.pingdingshan university,Pingdingshan, Henna ,467000,China School of chemistry and chemical engineering, jiangsu universityjiangsu,Zhenjiang,212013,China

会议类型: 国际会议

会议名称: 2011 Fourth International Conference on Intelligent Computation Technology and Automation(2011年第四届智能计算技术与自动化国际会议 ICICTA 2011)

会议地点: 深圳

会议语种:英文

页码: 821-823

在线出版日期: 2011-03-28（万方平台首次上网日期，不代表论文的发表时间）