Preparation and Structural Phase Transitions of Silver Palmitate

摘要：

Silver palmitate was prepared by chemical deposition method using palmitate acid, sodium hydroxide and silver nitrate as raw materials in water system. The structure and thermal properties of silver palmitate were characterized by SEM, XRD, FTIR, TG and DSC. The results show that silver palmitate has a good purity and well-defined layer structure with triclinic phase. TG and DSC curves demonstrate that silver palmitate decomposed at 230 and 250℃. One of the decomposed products at 230℃ is a free acid with melting point at 52℃. The endothermic peak at 120℃ attributes to the order-disorder phase transition. The three endothermic peaks at 159, 166 and 175℃ assign to reversible phase transitions among intermediate phases.

关键词： Silver Palmitate Chemical Deposition Method Preparation Structural Phase Transition

作者: Ya-ling Li Shui Wang Xu Zhang Xiao-ling Yang

作者单位: Beijing Key Laboratory of Printing & Packaging Materials and Technology, Beijing Institute of Graphi College of Chemical Engineering, Beijing University of Chemical and Technology,No.15, BeiSanhuan Don

会议类型: 国际会议

会议名称: 第二届多功能材料与结构国际会议

会议地点: 青岛

会议语种:英文

页码: 1647-1650

在线出版日期: 2009-10-09（万方平台首次上网日期，不代表论文的发表时间）