Synthesis and Characterization of NH4V(Gly)3(PO4)2.H2O
A new vanadium-glycine complex (NH4V(Gly)3(PO4)2.H2O) was synthesized in hydrothermal condition and characterized by XRD, FTIR, SEM and TG-DSC techniques. The results indicate that glycine and water exist in the crystal framework as ligand coordinating with vanadium. The SEM images show that the single crystals are homogeneous in crystal size and shape, and show a good crystalline performance. The size of crystals is about 20×20×20μm3. It has a certain potential of application in studying the relationships between the chemical and biological properties of vanadium compounds.
vanadium glycine hydrothermal synthesis ligand complez
Bo Wei Huiqun Cao Jianmin Sun Yujuan Lv
Chemistry and Chemical Engineering College Shenzhen University Shenzhen 518060,PR China State Key Laboratory of Inorganic Synthesis and Preparative Chemistry Jilin University Changchun 130
国际会议
北京
英文
1-3
2009-06-11(万方平台首次上网日期,不代表论文的发表时间)