One-Step Synthesis of Perovskite LaCrO3 Nanopowders by Mcrowave Induced Combustion of Metal Nitrate-Glycine Mizture Solution

摘要：

In the work, well-dispersed perovskite LaCrO3 powders with average crystallite size of about 16 nm have been synthesized by one step via microwave induced solution combustion reaction using glycine as fuel and correspondant nitrates asoxidants. The simutaneous thermogravity and differential thermal analysis (TG-DTA) were used to study the auto-combustion and thermal decomposition of the precursor. The effects of glycine-nitrate molar ratio (G/N) and heat-treatment temperature on the perovskite-phase formation and crystallite size of as-burnt powder were studied by powder X-ray diffractometry (XRD). The morphology and size of as-burnt powders were characterized by and transmission electron microscopy (TEM).

关键词： Microwave induced, Combustion synthesis LaCrO3 Perovskite Nanopowder Glycine

作者: Chen Weifan Li Yongxiu Gu Ziying

作者单位: School of Materials Science & Engineering, Nanchang University 330031, PR China Research Center for Research Center for Rare Earths & Micro/Nano Functional Materials, Nanchang University 330031, PR Ch Research Center for Rare Earths & Micro/Nano Functional Materials, Nanchang University 330031, PR Ch

会议类型: 国际会议

会议名称: The 8th International Coference on Measurement and Control of GranularMaterials(第八届国际粉体检测与控制学术会议)(MCGM 2009)

会议地点: 沈阳

会议语种:英文

页码: 132-135

在线出版日期: 2009-08-27（万方平台首次上网日期，不代表论文的发表时间）