Preparation of Titanate Nanotubes by Hydrothermal Method
Titanate nanotubes have been directly prepared by hydrothermally treating P25 powders in NaOH aqueous solution. Effect of calcination temperature on crystal phase, morphologies and specific surface area of the as-synthesized nanotubes has been investigated in detail. The Na2Ti3O7 tubular structure could be kept well even after calcination at 600 ℃ and began to transform to Na2Ti6O13 nanorods at around 645 ℃. The specific surface area of the as-synthesized nanotubes was 200.6 m2/g and reached to the maximum of 347.9 m:/g after calcination at 300℃ and then decreased sharply with the further increase of the calcination temperature.
titanate nanotube hydrothermal method
Dan-Ni YU Wen-Xiu LIU Jing MA Xiao-Guang QU Wen-Bin CAO Zhong-Ying ZHANG Jing-Hong MAO
Department of Inorganic Nonmetallic Materials, School of Materials Science and Engineering,University of Science and Technology Beijing, Beijing 100083, China
国际会议
10th International Symposium on Eco-Materials Processing and Design(第10届国际生态材料加工与设计研讨会)
西安
英文
687-890
2009-01-13(万方平台首次上网日期,不代表论文的发表时间)