Preparation of Nano Titanium Dioxide using Industrial Raw Material

In this paper, nano-sized titanium dioxide particles were prepared by homogeneous precipitation method using industrial TiOSO4 as raw material. The morphology, crystal structures and the crystal transformation were characterized using transmission electron microscopy (TEM),X-ray Diffraction (XRD), and thermogravimetry-differential thermogravimetric analyzer (TG-DTA) respectively. The impact factors on the production rate and the diameters of nano-TiO2 were investigated. The factors include the reaction temperature, the concentrations of reactants, the molar ratios of reactants, the reaction time, the calcination temperature, and the calcination time. The results indicated that nano anatase titanium dioxide in uniform phase could be obtained under a reaction temperature of 90℃, the concentration of riO2+ at 0.Smol/L, the reaction time of 4h, the ratio of CO(NH2)2 to TiOSO4 as 1:3, followed by a calcination period of 2h under 600℃,
homogeneous precipitation method TiO2 nanopowder anatase
Peixin Zhang Dongyun Zhang Qi Qiu Li Jing Xiangzhong Ren
School of Materials Science and Engineering,Xian University of Architecture and Technology,Xian 71 School of Materials Science and Engineering,Xian University of Architecture and Technology,Xian 71 School of Chemistry and Chemical Engineering,Shenzhen University,Shenzhen 518060,P.R.China
国际会议
2008国际粉体技术与应用论坛暨全国粉体产品与设备应用技术交流大会
北京
英文
129-139
2008-04-01(万方平台首次上网日期,不代表论文的发表时间)