Growth of Lead Oxide Nanorods by Electrochemical Reduction Method
A simple method to fabricate lead oxide nanorods by an electrochemical reduction was reported. In the experiment, the electrolyte was lead nitrate aqueous solution containing zirconium oxide chloride and titanium ( Ⅲ ) chloride solution. Stainless steel plate was employed as both cathode and substrate. The controlled current that was supplied by a DC power supply passed through the electrolyte to deposit lead oxide nanorods on the surface of stainless steel at room temperature. The yield of lead oxide nanorods was affected by the current density. So the impact of the current density on the yield of lead oxide nanorods was discussed in order to find the optimal current density for the fabrication of lead oxide nanorods. The as-synthesized products were characterized by SEM, TEM, EDS and XRD. The results of characterization indicated that the lead oxide nanorods were single crystals.
Lead oxide Nanorods Electrochemical reduction Current density
任鹏飞 邹小平 程进 张红丹 李飞 朱光 王茂发
北京信息工程学院传感技术研究中心,北京,100101;北京市传感器重点实验室,北京,100101
国际会议
第二届功能原料国际研讨会(The 2rd International Symposium on Functional Materials)
杭州
英文
902-905,931
2007-05-16(万方平台首次上网日期,不代表论文的发表时间)