Determination of Chlordane in Soil Around the Factory With QuEChERS-GC/MS

摘要：

A simple, fast, and inexpensive method was developed to analyze chlordane in soil with gas chromatography- mass spectrometry (GC-MS). The samples were extracted with acetone/hexane (1:1, v/v) followed by ultrasonic. After addition of primary secondary amine (PSA), the supernatant was transferred into a vial and ready for injection into GC-MS. GC-MS-SIM was employed to determinate chlordane in soil. Recoveries were in the range of 93％~101％. The coefficients of determination R<2> were above 0.999 in the range of 0.1～100mg/L. The concentrations of chlordane in the soils ranged from 0.079mg/kg to 2927.95mg/kg. In some samples, the value exceeded the normal of Environmental Protection Agency (USA).

关键词： Chlordanel QuEChERS PSA GC-MS-SIM soil

作者: Zhang Heli Pan Canping

作者单位: Department of Basic Science, Zhengzhou College of Animal Husbandry Engineering, Zhengzhou 450011, P. College of Science, China Agricultural University, Beijing 100094, P. R. China

会议类型: 国际会议

会议名称: 第三届“农药与环境安全国际学术研讨会暨第七届“植物化学保护和全球法律一体化国际研讨会(3rd International Symposium on Pesticide and Environmental Safety & 7th International Workshop on Crop Protection Chemistry and Regulatory Harmonization)

会议地点: 北京

会议语种:英文

页码: 259-262

在线出版日期: 2007-10-09（万方平台首次上网日期，不代表论文的发表时间）