Refinement of Hexabenzylhexaazaisowurtzitane (HBIW) by Mixed Solvent
Hexabenzylhexaazaisowurtzitane (HBIW) is the precursor to hexanitrohexaazaisowurtzitane (HNIW)-the most powerful high energy density explosive ever tested. In this paper, comparing the recrystallization rate of HBIW on different concentrations of DMF-Acetone solution, it is showed that the optimum ratio of mixed solvents is 30％ DMF, 70％ acetone (quality percentage; the volume ratio of solute and solvent was about 1:6, but carry on recrystallization with the pure acetone, the volume ratio of solute and solvent was about 1:12. This, to a great extent, saved the solvent of recrystallization, and improved recrystallization efficiency greatly.
hexabenzylhexaazaisowurtzitane (HBIW) recrystallization mixed solvent
WANG Ruifang SHI Yanshan CHEN Shusen JIN Shaohua
School of Material Science and Technology, Beijing Institute of Technology, Beijing 100081, China
国际会议
西安
英文
34-35
2007-10-23（万方平台首次上网日期，不代表论文的发表时间）