Synthesis of BaFBr Nanoparticles from Microemusion
BaFBr nanoparticles were synthesized by cetyltrimethylammonium bromide (CTAB)/2-octanol/water microemusion systems. X-ray diffraction (XRD) analysis shows that depending on the molar starting ratio of NH4F to NH4Br, stoichiometric BaFBr with or without a BaF2 phase is obtained. As the ratio of NH4F to NH4Br reduced from 1.0:1.0 to 1.0:4.0, the product forms pure BaFBr. Calculations using Debye-Scherrer equation from line widths of the XRD and images of transmission electron microscopy (TEM) show particle sizes of less than 100nm.
nanoparticle BaFBr synthesis microemusion XRD
Xianguo Meng Yongsheng Wang
Key Laboratory of Luminescence and Optical Information,Ministry of Education,Institute of Optoelectronic Technology,Beijing Jiaotong University,Beijing 100044,China
国际会议
成都
英文
2007-11-19(万方平台首次上网日期,不代表论文的发表时间)