Study on the Gel Point of the Precursor Sol of Mullite Fiber
Using water as disperse medium, aluminum nitrate (AN), aluminum isopropoxide (AIP) and tetraethoxysilane (TEOS) as raw materials, polyvinylpyrrolidone (PVP) as modifier, the precursor sol of mullite fiber was synthesized by sol-gel method. Through dynamic theological measurements, the gel points of the different systems were determined according to Chambon-Winter (CW) criterion. The influences of PVP and aging temperature on the gel point of the precursor sol were also investigated. They exert great influences on the gel point of the specific system. From these work, it may provide scientific basis for the preparation of the continuous mullite fiber.
mullite fiber precursor sol gel point rheological measurement
LIU Meirong CHEN Xintuo GU Liqin GU Lixia
State Key Laboratory for Modification of Chemical Fibers and Polymer Materials, Donghua University, Shanghai 201620, P. R. China
国际会议
上海
英文
458-460
2007-10-15(万方平台首次上网日期,不代表论文的发表时间)