Study On Phase Transfer Catalytic Synthesis of N,N-Diethylaniline with 1,4,7,10,13,16-Hexaoxacyclooctadecane

摘要：

　　Using 1,4,7,10,13,16-Hexaoxacyclooctadecane as phase transfer catalyst, N,N-Diethylaniline is synthesized by reaction of aniline with bromoethane under atmospheric pressure.The factors affecting the yield of the target product have been studied.The optimal reaction conditions are molar ratio of aniline to bromoethane, 1:1.50;35× 10-2 sodium hydroxide solution, 45ml;catalyst, 0.8g;reaction temperature, 55℃;reaction time, 4h;under normal atmosphere.The yield of N,N-diethylaniline is 73.1%.

关键词： 1,4,7,10,13,16-Hexaoxacyclooctadecane Phase Transfer Catalyst N,N-Diethylaniline

作者: Qingwei TIAN

作者单位: Department of Enuironmental Science and Chemical Engineering, Dalian Jiaotong University, Liaoning, Dalian, 116028, China

会议类型: 国内会议

会议名称: 2010中国可再生能源科技发展大会

会议地点: 北京

会议语种:英文

页码: 264-269

在线出版日期: 2010-12-18（万方平台首次上网日期，不代表论文的发表时间）